In microelectronic industry, thin polymer layers are one of the more commonly used product constituents. Examples are glue layers, coatings, and dielectric layers. The thicknesses of these films vary from a few tens of nanometers to over a hundred micrometers. Since at film thicknesses below the thermal and mechanical properties start to deviate from those in the bulk, adequate characterization techniques are required. In the present paper we will report the results of an extensive literature search on the state-of-the-art of thermo-mechanical thin film characterization methods, such as the substrate curvature test, nanoindentation technique, bulge test, and impulsive stimulated thermal scattering.
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Technology Review
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, B.
, Liu
, Q. Z.
, and Brongo
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, 2000, “Mechanical Property Measurement of Thin Polymeric-Low Dielectric-Constant Films Using Bulge Testing Method
,” Appl. Phys. Lett.
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, pp. 2008
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.34.
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, M. K.
, and Nix
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, 1992, “Analysis of the Accuracy of the Bulge Test in Determining the Mechanical Properties of Thin Films
,” J. Mater. Res.
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, pp. 1553
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, C.
, Delobelle
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, Lexcellent
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, S.
, and Tobushi
, H.
, 2000, “Analysis of the Mechanical Behavior of Shape Memory Polymer Membranes by Nanoindentation, Bulging and Point Membrane Deflection Tests
,” Thin Solid Films
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, pp. 156
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.36.
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, J. J.
, and Nix
, W. D.
, 1992, “A New Bulge Test Technique for the Determination of Young’s Modulus and Poisson’s Ratio of Thin Films
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, T. T.
, and Liu
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, A. R.
, Rogers
, J. A.
, Nelson
, K. A.
, and Mordechai
, R.
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, Hau
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, J. K.
, Hau
, C. S.
, Lee
, P. M.
, et al., 1995, “Characterization of 6FDA-APBP Polyimide Films Through Impulsive Stimulated Thermal Scattering
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, J. A.
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, and Nelson
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, pp. 523
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.45.
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, A. R.
, Rogers
, J. A.
, and Nelson
, K. A.
, 1992, “Real-Time Optical Characterization of Surface Acoustic Modes of Polyimide Thin-Film Coatings
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, pp. 2823
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, T.
, Kotera
, M.
, Inayoshi
, N., et al., 2000, “Residual Stress and Microstructures of Aromatic Polyimide With Different Imidization Processes
,” Polymer
0032-3861, 41
, pp. 6913
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.47.
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, J. M.
, Chang
, S. M.
, and Muramatsu
, H.
, 1999, “Monitoring Changes in the Viscoelastic Properties of Thin Polymer Films by the Quartz Crystal Resonator
,” Polymer
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, pp. 3291
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, V. V.
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, N.
, and Tsukruk
, V. V.
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, pp. 603
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.49.
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, A. K.
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, R. P.
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, R. J.
, and Challis
, R. E.
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, V.
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, M.
, and Legras
, R.
, 2001, “Supported Dynamic Mechanical Thermal Analysis: An Easy, Powerful and Very Sensitive Techniq to Assess Thermal Properties of Polymer, Coating and Even Nanocoating
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0032-3861, 42
, pp. 5327
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, A.
, 1995, “Generation and Relief of Stress in Ceramic Films
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, and Senturia
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, J. A.
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, and Nelson
, K. A.
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