Abstract

This work investigates the effect of pack boriding time and temperature on the wear and corrosion resistance of AISI H13 tool steel. Steel samples were pack borided at 900 and 1000°C for periods of 2 and 4 h; followed by non-abrasive fixed-ball microwear tests on borided and non-borided samples. The corrosion resistance was evaluated by potentiodynamic polarization tests in HCl 0.1 M. High hardness layers were formed on the samples for all treatment conditions employed. The layer's properties, such as hardness, thickness, layer/substrate interface morphology, and phases formed, were influenced by steel composition. For AISI H13 steel, which has a larger amount of alloying elements than carbon steel, the formed layers were hard, thin, with a smoother interface. For all treatment conditions, the presence of Fe2B, FeB, and CrB were identified. The wear and corrosion resistance of borided samples was significantly increased. The best results were obtained for samples borided at 1000°C.

References

1.
Singhal
,
S. C.
, “
A Hard Diffusion Boride Coating for Ferrous Materials
,”
Thin Solid Films
, Vol.
45
, No.
2
,
1977
, pp.
321
329
. https://doi.org/10.1016/0040-6090(77)90265-6
2.
Habig
,
K.-H.
and
Chatterjjee-Fischer
,
R.
, “
Wear Behaviour of Boride Layers on Alloyed Steels
,”
Tribol. Int.
, Vol.
14
, No.
4
,
1981
, pp.
209
215
. https://doi.org/10.1016/0301-679X(81)90043-8
3.
Fichtl
,
W.
, “
Boronizing and its Practical Applications
,”
Mater. Eng.
, Vol.
2
, No.
6
,
1981
, pp.
276
286
. https://doi.org/10.1016/0261-3069(81)90034-0
4.
Dearnley
,
P. A.
and
Bell
,
T.
, “
Engineering the Surface With Boron Based Materials
,”
Surf. Eng.
, Vol.
1
, No.
3
,
1985
, pp.
203
217
. https://doi.org/10.1179/sur.1985.1.3.203
5.
Sinha
,
A. K.
, “
Boriding (Boronizing)
,”
ASM Handbook
, Vol.
4
,
ASM International
,
Materials Park, OH
,
1991
.
6.
Selçuk
,
A. B.
,
Ipek
,
R.
,
Karamiş
,
M. B.
, and
Kuzucu
,
V.
, “
An Investigation on Surface Properties of Treated Low Carbon and Alloyed Steels (Boriding and Carburizing)
,”
J. Mater. Process. Technol.
, Vol.
103
, No.
2
,
2000
, pp.
310
317
. https://doi.org/10.1016/S0924-0136(99)00488-4
7.
Ozbek
,
I.
and
Bindal
,
C.
, “
Mechanical Properties of Boronized AISI W4 Steel
,”
Surf. Coatings Technol.
, Vol.
154
, No.
1
,
2002
, pp.
14
20
. https://doi.org/10.1016/S0257-8972(01)01409-8
8.
Martini
,
C.
,
Palombarini
,
G.
,
Poli
,
G.
, and
Prandstraller
,
D.
, “
Sliding and Abrasive Wear Behaviour of Boride Coatings
,”
Wear
, Vol.
256
, No.
6
,
2004
, pp.
608
613
. https://doi.org/10.1016/j.wear.2003.10.003
9.
Petrova
,
R. S.
,
Suwattananont
,
N.
, and
Samardzic
,
V.
, “
The Effect of Boronizing on Metallic Alloys for Automotive Applications
,”
J. Mater. Eng. Perform.
, Vol.
17
, No.
3
,
2008
, pp.
340
345
. https://doi.org/10.1007/s11665-008-9228-2
10.
Oliveira
,
C. K. N.
,
Casteletti
,
L. C.
,
Lombardi Neto
,
A.
,
Totten
,
G. E.
, and
Heck
,
S. C.
, “
Production and Characterization of Boride Layers on AISI D2 Tool Steel
,”
Vacuum
, Vol.
84
, No.
6
,
2010
, pp.
792
796
. https://doi.org/10.1016/j.vacuum.2009.10.038
11.
Fernandes
,
F. A. P.
,
Heck
,
S. C.
,
Totten
,
G. E.
, and
Casteletti
,
L. C.
, “
Wear Evaluation of Pack Boronized AISI 1060 Steel
,”
Mater. Perform. Character.
, Vol.
2
, No.
1
,
2013
, pp.
58
66
. https://doi.org/10.1520/MPC20120009
12.
Martini
,
C.
,
Palombarini
,
G.
, and
Carbucicchio
,
M.
, “
Mechanism of Thermochemical Growth of Iron Borides on Iron
,”
J. Mater. Sci.
, Vol.
39
, No.
3
,
2004
, pp.
933
937
. https://doi.org/10.1023/B:JMSC.0000012924.74578.87
13.
Shirokov
,
V. V.
,
Kitsak
,
M. I.
,
Rudkovs'kyi
,
E. T.
, and
Arendar
,
L. A.
, “
Formation and Properties of Diffusion Coatings Applied to Steels by Boronizing in Melts
,”
Mater. Sci.
, Vol.
35
, No.
2
,
1999
, pp.
245
251
. https://doi.org/10.1007/BF02359986
14.
Genel
,
K.
, “
Boriding Kinetics of H13 Steel
,”
Vacuum
, Vol.
80
, No.
5
,
2006
, pp.
451
457
. https://doi.org/10.1016/j.vacuum.2005.07.013
15.
Davis
,
J. R.
,
Corrosion: Understanding the Basics
,
ASM International
,
Materials Park, OH
,
2000
.
This content is only available via PDF.
You do not currently have access to this content.